Factual error: Ole and all the Thrush baddies call the missing chemical component a "catalyzer," repeating the term throughout the episode. This was a scriptwriter's error, which only David McCallum, to his credit, corrected: he had Illya say "catalyst," which is what the writer meant. "Catalyzer" isn't a word.
Continuity mistake: The table with the code papers resting on it is smashed during the fight in the final act. Yet, when the fight is nearly over, the table has restored itself with the papers still on it, only to be squashed all over again.
00:45:00 - 00:47:05Jean G
Continuity mistake: The Thrush assassins have an armed golf cart (with a machine gun that handily spews both flames and bullets at the same time). When the cart overturns, the two men fall into a sand trap and tumble several feet away from the vehicle. In the very next shot, they're lying right beside the cart again.
Continuity mistake: Solo picks up a book, The History of Pacifism, and shows it to Illya, holding it at the bottom. Cut to a close-up insert and his fingers have instantly migrated up to the middle of the book. Cut back to the wider shot, and he's no longer holding the book at all. It's back on the table.
Factual error: The jailed student protestors are dancing in their cell to a jazzy tune. But they have no radio or record player - just one guy with a guitar. They seem to have conjured the accompanying saxophone, jazz clarinets and percussion section out of thin air.
Factual error: Illya leaps onto the rope in the monastery tower, causing the bell to ring. After sliding down the rope to the floor, he then identifies the tone as "B Major 7th." But the musically-literate Illya should know better. B Major 7th is a chord (B, D-sharp, F-sharp, A-sharp), not a single note.
Plot hole: U.N.C.L.E.'s pen communicators worked much like modern cell phones: when one agent called another, they "rang" with a 2-tone signal. For some reason in this episode, Solo's pen, which isn't on an open circuit, transmits Illya's voice without ringing first. It signals normally a few scenes later, though.
00:27:55 - 00:34:15Jean G
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