Harry: Looks like I came just in time.
Spider-man: Yeah, few seconds ago wouldn't have been so bad either.
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During the final fight scene, Spiderman is talking to Mary Jane while Harry is flying around. There is a shot of the Sandman about to clap his hands together around Harry. As the scene cuts to Spiderman taking off to save Harry and cuts back, Sandman's hands are much farther apart than they were before the cut.
During the scene on the bridge where MJ breaks up with Peter, MJ's hair is tied behind her head with a few wisps hanging down and her ears visible whenever she is shown from behind. However, whenever MJ is shown in her own close-up during the same conversation, her hair is down loosely and her ears are completely covered up.
In the scene where Peter asks Harry to help rescue M. J. (from Venom and Sandman), a sitting chair appears to the left of the painting of Harry's father in the last shot of Harry. There was no chair in the other shots of this scene. The sitting chair was by that painting for all of the movie except those few shots.